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Conjugate additions of carbon nucleo...
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Zhang, Ming.
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Conjugate additions of carbon nucleophiles to cyclopentadienones .
紀錄類型:
書目-電子資源 : Monograph/item
正題名/作者:
Conjugate additions of carbon nucleophiles to cyclopentadienones ./
作者:
Zhang, Ming.
面頁冊數:
236 p.
附註:
Source: Dissertation Abstracts International, Volume: 67-10, Section: B, page: 5766.
Contained By:
Dissertation Abstracts International67-10B.
標題:
Chemistry, Organic. -
電子資源:
http://pqdd.sinica.edu.tw/twdaoapp/servlet/advanced?query=3237857
ISBN:
9780542928505
Conjugate additions of carbon nucleophiles to cyclopentadienones .
Zhang, Ming.
Conjugate additions of carbon nucleophiles to cyclopentadienones .
- 236 p.
Source: Dissertation Abstracts International, Volume: 67-10, Section: B, page: 5766.
Thesis (Ph.D.)--Case Western Reserve University, 2007.
The optimization of Fe(CO)5 promoted cyclocarbonylation of temporary silicon-tethered diynes is described. Various monomeric cyclopentadienones with hydroxyl substituents were produced in good yields as a result.
ISBN: 9780542928505Subjects--Topical Terms:
516206
Chemistry, Organic.
Conjugate additions of carbon nucleophiles to cyclopentadienones .
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Source: Dissertation Abstracts International, Volume: 67-10, Section: B, page: 5766.
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Thesis (Ph.D.)--Case Western Reserve University, 2007.
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The optimization of Fe(CO)5 promoted cyclocarbonylation of temporary silicon-tethered diynes is described. Various monomeric cyclopentadienones with hydroxyl substituents were produced in good yields as a result.
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Conjugate additions of carbon nucleophiles to these cyclopentadienones and their corresponding protected derivatives were studied. Chelate Mg coordinated cyclopentadienone intermediates were proposed to explain the resulting regio- and stereochemistry. For the mono-protected cyclopentadienone substrates, a hydroxyl-delivery mechanism was proposed.
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An unexpected cyclopropanation was observed during the conjugate additions of Grignard reagents to TBS protected hydroxyalkyl-substituted cyclopentadienones. It was prevented after replacing the TBS protecting group with methyl.
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