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Efforts toward the Synthesis and Dev...

Gafur, Sayed Habibul.

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Efforts toward the Synthesis and Development of Oxadiazinones as Organocatalysts, and the Development of Synthetic Methods for the Preparation of Sulfinate Esters and Sulfinamides.

Record Type:	Electronic resources : Monograph/item
Title/Author:	Efforts toward the Synthesis and Development of Oxadiazinones as Organocatalysts, and the Development of Synthetic Methods for the Preparation of Sulfinate Esters and Sulfinamides./
Author:	Gafur, Sayed Habibul.
Published:	Ann Arbor : ProQuest Dissertations & Theses, : 2018,
Description:	159 p.
Notes:	Source: Masters Abstracts International, Volume: 80-01.
Contained By:	Masters Abstracts International80-01.
Subject:	Chemistry. -
Online resource:	http://pqdd.sinica.edu.tw/twdaoapp/servlet/advanced?query=10790196
ISBN:	9780438108233

Efforts toward the Synthesis and Development of Oxadiazinones as Organocatalysts, and the Development of Synthetic Methods for the Preparation of Sulfinate Esters and Sulfinamides.
Gafur, Sayed Habibul.

Efforts toward the Synthesis and Development of Oxadiazinones as Organocatalysts, and the Development of Synthetic Methods for the Preparation of Sulfinate Esters and Sulfinamides. - Ann Arbor : ProQuest Dissertations & Theses, 2018 - 159 p.

Source: Masters Abstracts International, Volume: 80-01.

Thesis (M.S.)--Illinois State University, 2018.

This item must not be sold to any third party vendors.

This body of research is composed of three independent parts. In the first part, which is the subject matter of chapter I, organocatalytic activity of oxadiazinones in chlorination reaction of hydrocinnamaldehyde was investigated. It was found that depending on the structure, oxadiazinones can efficiently catalyze chlorination of hydrocinnamaldehyde, although with poor enantioselectivity under the reaction conditions. Details of this investigation are reported in chapter I. Second part of the research was focused on synthesis of alpha amino acid based sulfInamides and their application as Lewis basic organocatalyst in allylation of hydrazones. Details of the investigation of allylation of isobutyraldehyde derived benzoylhydrazone using allyltrichlorosilane is reported in chapter II. Finally in chapter III which describes the third part of the research, development of a method suitable for high throughput synthesis of sulfinate esters via an O-acylisourea intermediate is reported.

ISBN: 9780438108233Subjects--Topical Terms:

516420
Chemistry.

Efforts toward the Synthesis and Development of Oxadiazinones as Organocatalysts, and the Development of Synthetic Methods for the Preparation of Sulfinate Esters and Sulfinamides.
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300 $a 159 p.
500 $a Source: Masters Abstracts International, Volume: 80-01.
500 $a Publisher info.: Dissertation/Thesis.
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502 $a Thesis (M.S.)--Illinois State University, 2018.
506 $a This item must not be sold to any third party vendors.
520 $a This body of research is composed of three independent parts. In the first part, which is the subject matter of chapter I, organocatalytic activity of oxadiazinones in chlorination reaction of hydrocinnamaldehyde was investigated. It was found that depending on the structure, oxadiazinones can efficiently catalyze chlorination of hydrocinnamaldehyde, although with poor enantioselectivity under the reaction conditions. Details of this investigation are reported in chapter I. Second part of the research was focused on synthesis of alpha amino acid based sulfInamides and their application as Lewis basic organocatalyst in allylation of hydrazones. Details of the investigation of allylation of isobutyraldehyde derived benzoylhydrazone using allyltrichlorosilane is reported in chapter II. Finally in chapter III which describes the third part of the research, development of a method suitable for high throughput synthesis of sulfinate esters via an O-acylisourea intermediate is reported.
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