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Design, synthesis, characterization,...
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Lanni, Laura M.
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Design, synthesis, characterization, and evaluation of boronate ester-linked porous materials: Covalent organic frameworks and polymers of intrinsic microporosity.
紀錄類型:
書目-電子資源 : Monograph/item
正題名/作者:
Design, synthesis, characterization, and evaluation of boronate ester-linked porous materials: Covalent organic frameworks and polymers of intrinsic microporosity./
作者:
Lanni, Laura M.
出版者:
Ann Arbor : ProQuest Dissertations & Theses, : 2010,
面頁冊數:
200 p.
附註:
Source: Dissertation Abstracts International, Volume: 72-02, Section: B, page: 8970.
Contained By:
Dissertation Abstracts International72-02B.
標題:
Organic chemistry. -
電子資源:
http://pqdd.sinica.edu.tw/twdaoapp/servlet/advanced?query=3433161
ISBN:
9781124384313
Design, synthesis, characterization, and evaluation of boronate ester-linked porous materials: Covalent organic frameworks and polymers of intrinsic microporosity.
Lanni, Laura M.
Design, synthesis, characterization, and evaluation of boronate ester-linked porous materials: Covalent organic frameworks and polymers of intrinsic microporosity.
- Ann Arbor : ProQuest Dissertations & Theses, 2010 - 200 p.
Source: Dissertation Abstracts International, Volume: 72-02, Section: B, page: 8970.
Thesis (Ph.D.)--University of South Carolina, 2010.
An array of porous boronate ester-linked materials is presented here. Beginning with evaluation of a series of alkylated covalent organic frameworks (COFs), insight into the influence of alkylation in the hexagonal COF pores on the hydrolytic stability of the B-O linkages led to development of a family of hybrid COFs (HCOFs). These HCOFs were made by incorporating a gradual ladder of alkylation into the COF pores and provided a synthetic method to dial in stability along with porosity for specific COF applications. Parallel research resulted in a new COF with incorporated phthalocyanine groups (CuPC-COF) which could lead to future semiconducting thin films. The synthetic strategy to produce an octahydroxy-phthalocyanine monomer and the typical COF characterizations of PXRD and gas uptake are reported.
ISBN: 9781124384313Subjects--Topical Terms:
523952
Organic chemistry.
Design, synthesis, characterization, and evaluation of boronate ester-linked porous materials: Covalent organic frameworks and polymers of intrinsic microporosity.
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Design, synthesis, characterization, and evaluation of boronate ester-linked porous materials: Covalent organic frameworks and polymers of intrinsic microporosity.
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Source: Dissertation Abstracts International, Volume: 72-02, Section: B, page: 8970.
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An array of porous boronate ester-linked materials is presented here. Beginning with evaluation of a series of alkylated covalent organic frameworks (COFs), insight into the influence of alkylation in the hexagonal COF pores on the hydrolytic stability of the B-O linkages led to development of a family of hybrid COFs (HCOFs). These HCOFs were made by incorporating a gradual ladder of alkylation into the COF pores and provided a synthetic method to dial in stability along with porosity for specific COF applications. Parallel research resulted in a new COF with incorporated phthalocyanine groups (CuPC-COF) which could lead to future semiconducting thin films. The synthetic strategy to produce an octahydroxy-phthalocyanine monomer and the typical COF characterizations of PXRD and gas uptake are reported.
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The newest materials produced are porous yet amorphous and are the first family of boronate ester-linked polymers of intrinsic microporosity (PIMs). This family utilized the kink in a spirobisindane bis-diol monomer along with linear and trigonal boronic acids to produce amorphous solids which are intrinsically microporous. The potential of these materials to form permeable membranes and gas storage/separation devices, along with an abundant list of alternative commercially available monomers, warrant further development and testing of these boronate ester-linked PIMs.
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