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Synthesis and surface chemistry of Z...

Gupta, Anurag.

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Synthesis and surface chemistry of Zinc Oxide nanowires for chemical sensor applications.

Record Type:	Electronic resources : Monograph/item
Title/Author:	Synthesis and surface chemistry of Zinc Oxide nanowires for chemical sensor applications./
Author:	Gupta, Anurag.
Description:	128 p.
Notes:	Source: Dissertation Abstracts International, Volume: 75-08(E), Section: B.
Contained By:	Dissertation Abstracts International75-08B(E).
Subject:	Engineering, Materials Science. -
Online resource:	http://pqdd.sinica.edu.tw/twdaoapp/servlet/advanced?query=3620100
ISBN:	9781303897986

Synthesis and surface chemistry of Zinc Oxide nanowires for chemical sensor applications.
Gupta, Anurag.

Synthesis and surface chemistry of Zinc Oxide nanowires for chemical sensor applications. - 128 p.

Source: Dissertation Abstracts International, Volume: 75-08(E), Section: B.

Thesis (Ph.D.)--The University of Alabama, 2014.

The research work in this dissertation comprises of synthesis and functionalization of high quality ZnO nanowires for highly sensitive and selective p-nitrophenol vapor sensor. High-quality ZnO nanowires were synthesized through a vapor-liquid-solid process in a customized chemical vapor deposition furnace. Scanning electron microscopy, transmission electron microscopy, x-ray diffraction, and energy dispersive x-ray spectroscopy were used to characterize morphology, crystal structure and composition. Surface functionalization behavior of pristine ZnO nanowires was tested by oleic acid as a model compound and the surface modification was studied using surface sensitive techniques of Raman and FT-IR spectroscopies. Surface functionalization of ZnO nanowires with optically active 1-pyrenebutyric acid was investigated. A 1-pyrenebutyric acid compound was grafted on a solid-state ZnO nanowires backbone. Optical and electrical properties of this heterostructure were determined through fluorescence and I-V measurements, respectively. Two distinct approaches for device fabrication were tested for integrated system development and validation of sensor operation. A single nanowire device and a multi-nanowire array device were successfully fabricated.

ISBN: 9781303897986Subjects--Topical Terms:

1017759
Engineering, Materials Science.

Synthesis and surface chemistry of Zinc Oxide nanowires for chemical sensor applications.
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245 1 0 $a Synthesis and surface chemistry of Zinc Oxide nanowires for chemical sensor applications.
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500 $a Source: Dissertation Abstracts International, Volume: 75-08(E), Section: B.
500 $a Adviser: Bruce C. Kim.
502 $a Thesis (Ph.D.)--The University of Alabama, 2014.
520 $a The research work in this dissertation comprises of synthesis and functionalization of high quality ZnO nanowires for highly sensitive and selective p-nitrophenol vapor sensor. High-quality ZnO nanowires were synthesized through a vapor-liquid-solid process in a customized chemical vapor deposition furnace. Scanning electron microscopy, transmission electron microscopy, x-ray diffraction, and energy dispersive x-ray spectroscopy were used to characterize morphology, crystal structure and composition. Surface functionalization behavior of pristine ZnO nanowires was tested by oleic acid as a model compound and the surface modification was studied using surface sensitive techniques of Raman and FT-IR spectroscopies. Surface functionalization of ZnO nanowires with optically active 1-pyrenebutyric acid was investigated. A 1-pyrenebutyric acid compound was grafted on a solid-state ZnO nanowires backbone. Optical and electrical properties of this heterostructure were determined through fluorescence and I-V measurements, respectively. Two distinct approaches for device fabrication were tested for integrated system development and validation of sensor operation. A single nanowire device and a multi-nanowire array device were successfully fabricated.
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650 4 $a Engineering, Materials Science. $3 1017759
650 4 $a Chemistry, Inorganic. $3 517253
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710 2 $a The University of Alabama. $b Materials Science. $3 3168986
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