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Processing of lead magnesium niobate...

Gu, Huiming.

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Processing of lead magnesium niobate -lead titanate by a novel coating approach.

Record Type:	Electronic resources : Monograph/item
Title/Author:	Processing of lead magnesium niobate -lead titanate by a novel coating approach./
Author:	Gu, Huiming.
Description:	153 p.
Notes:	Source: Dissertation Abstracts International, Volume: 64-11, Section: B, page: 5718.
Contained By:	Dissertation Abstracts International64-11B.
Subject:	Engineering, Materials Science. -
Online resource:	http://pqdd.sinica.edu.tw/twdaoapp/servlet/advanced?query=3112648

Processing of lead magnesium niobate -lead titanate by a novel coating approach.
Gu, Huiming.

Processing of lead magnesium niobate -lead titanate by a novel coating approach. - 153 p.

Source: Dissertation Abstracts International, Volume: 64-11, Section: B, page: 5718.

Thesis (Ph.D.)--Drexel University, 2003.

Pb(Mg1/3Nb2/3)O3-PbTiO3 (PMN-PT) is an important ferroelectric material that has outstanding room temperature dielectric constant and electro-mechanical coefficient. Unlike most other ferroelectric materials, PMN-PT is difficult to prepare because of the formation of unwanted pyrochlore phase. Many methods of PMN-PT preparation have been developed to overcome this problem over the past decades. The remaining major problems for these methods are the high sintering temperature of 1200°C and the complex processing steps. In this thesis, a new coating method is introduced for PMN-PT processing. This method involves coating Mg(OH) 2 on the surface of Nb2O5 particles to increase the mixing of chemical components and enhance the complete transformation from pyrochlore phase to perovskite phase. With this method, the processing is simplified to only one-step calcination for PMN-PT powder preparation and one-step sintering for PMN-PT dense part preparation. At the same time, the sintering temperature is decreased to 1000°C. To gain fundamental understanding on the colloidal coating process, a modified SAK simulation model was developed. In powder processing, it was shown that smaller particle size and better powder configurations were the reasons for eliminating pyrochlore phase. On the other hand, smaller particle size and reactive sintering are responsible for the lower temperature sintering. Finally, processing optimization study showed that 0--2 at.% PbO excess is the ideal composition for high quality PMN-PT preparation.Subjects--Topical Terms:

1017759
Engineering, Materials Science.

Processing of lead magnesium niobate -lead titanate by a novel coating approach.
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035 $a (UnM)AAI3112648
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100 1 $a Gu, Huiming. $3 1952166
245 1 0 $a Processing of lead magnesium niobate -lead titanate by a novel coating approach.
300 $a 153 p.
500 $a Source: Dissertation Abstracts International, Volume: 64-11, Section: B, page: 5718.
500 $a Advisers: Wei-Heng Shih; Wan Y. Shih.
502 $a Thesis (Ph.D.)--Drexel University, 2003.
520 $a Pb(Mg1/3Nb2/3)O3-PbTiO3 (PMN-PT) is an important ferroelectric material that has outstanding room temperature dielectric constant and electro-mechanical coefficient. Unlike most other ferroelectric materials, PMN-PT is difficult to prepare because of the formation of unwanted pyrochlore phase. Many methods of PMN-PT preparation have been developed to overcome this problem over the past decades. The remaining major problems for these methods are the high sintering temperature of 1200°C and the complex processing steps. In this thesis, a new coating method is introduced for PMN-PT processing. This method involves coating Mg(OH) 2 on the surface of Nb2O5 particles to increase the mixing of chemical components and enhance the complete transformation from pyrochlore phase to perovskite phase. With this method, the processing is simplified to only one-step calcination for PMN-PT powder preparation and one-step sintering for PMN-PT dense part preparation. At the same time, the sintering temperature is decreased to 1000°C. To gain fundamental understanding on the colloidal coating process, a modified SAK simulation model was developed. In powder processing, it was shown that smaller particle size and better powder configurations were the reasons for eliminating pyrochlore phase. On the other hand, smaller particle size and reactive sintering are responsible for the lower temperature sintering. Finally, processing optimization study showed that 0--2 at.% PbO excess is the ideal composition for high quality PMN-PT preparation.
590 $a School code: 0065.
650 4 $a Engineering, Materials Science. $3 1017759
650 4 $a Chemistry, Inorganic. $3 517253
690 $a 0794
690 $a 0488
710 2 0 $a Drexel University. $3 1018434
773 0 $t Dissertation Abstracts International $g 64-11B.
790 1 0 $a Shih, Wei-Heng, $e advisor
790 1 0 $a Shih, Wan Y., $e advisor
790 $a 0065
791 $a Ph.D.
792 $a 2003
856 4 0 $u http://pqdd.sinica.edu.tw/twdaoapp/servlet/advanced?query=3112648