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Synthesis and characterization of bi...

Budhi, Sridhar.

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Synthesis and characterization of binary titania-silica mixed oxides.

Record Type:	Language materials, printed : Monograph/item
Title/Author:	Synthesis and characterization of binary titania-silica mixed oxides./
Author:	Budhi, Sridhar.
Description:	57 p.
Notes:	Source: Masters Abstracts International, Volume: 49-02, page: 1190.
Contained By:	Masters Abstracts International49-02.
Subject:	Chemistry, Inorganic. -
Online resource:	http://pqdd.sinica.edu.tw/twdaoapp/servlet/advanced?query=1482791
ISBN:	9781124315201

Synthesis and characterization of binary titania-silica mixed oxides.
Budhi, Sridhar.

Synthesis and characterization of binary titania-silica mixed oxides. - 57 p.

Source: Masters Abstracts International, Volume: 49-02, page: 1190.

Thesis (M.S.)--University of South Dakota, 2010.

A series of binary titania-silica mixed oxides were synthesized by the sol-gel method at room temperature. The mixed oxides were prepared that involved the hydrolysis of titanium isopropoxide and tetraethylorthosilicate (TEOS) by co-solvent induced gelation usually in acidic media. The resulting gels were dried, calcined and then characterized by powder X-ray diffractometric studies, nitrogen sorption studies (at 77K), diffuse reflectance spectroscopy, Raman microscopy and transmission electron microscopic studies. The nitrogen sorption studies indicate that the specific surface areas, pore volume, pore diameter and pore size distribution of the mixed oxides were substantially enhanced when non-polar solvents such as toluene, p-xylene or mesitylene were added as co-solvents to the synthesis gel. Transmission electron microscopic (TEM) studies confirm the results obtained from the nitrogen sorption studies. Our results indicate that we can obtain binary metal oxides possessing high surface area and large pore volumes with tunable pore size distribution at room temperature. Photocatalytic evaluation of the mixed oxides is currently in progress.

ISBN: 9781124315201Subjects--Topical Terms:

517253
Chemistry, Inorganic.

Synthesis and characterization of binary titania-silica mixed oxides.
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020 $a 9781124315201
035 $a (UMI)AAI1482791
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040 $a UMI $c UMI
100 1 $a Budhi, Sridhar. $3 1683993
245 1 0 $a Synthesis and characterization of binary titania-silica mixed oxides.
300 $a 57 p.
500 $a Source: Masters Abstracts International, Volume: 49-02, page: 1190.
500 $a Adviser: Ranjit Koodali.
502 $a Thesis (M.S.)--University of South Dakota, 2010.
520 $a A series of binary titania-silica mixed oxides were synthesized by the sol-gel method at room temperature. The mixed oxides were prepared that involved the hydrolysis of titanium isopropoxide and tetraethylorthosilicate (TEOS) by co-solvent induced gelation usually in acidic media. The resulting gels were dried, calcined and then characterized by powder X-ray diffractometric studies, nitrogen sorption studies (at 77K), diffuse reflectance spectroscopy, Raman microscopy and transmission electron microscopic studies. The nitrogen sorption studies indicate that the specific surface areas, pore volume, pore diameter and pore size distribution of the mixed oxides were substantially enhanced when non-polar solvents such as toluene, p-xylene or mesitylene were added as co-solvents to the synthesis gel. Transmission electron microscopic (TEM) studies confirm the results obtained from the nitrogen sorption studies. Our results indicate that we can obtain binary metal oxides possessing high surface area and large pore volumes with tunable pore size distribution at room temperature. Photocatalytic evaluation of the mixed oxides is currently in progress.
590 $a School code: 0203.
650 4 $a Chemistry, Inorganic. $3 517253
650 4 $a Chemistry, Physical. $3 560527
650 4 $a Nanoscience. $3 587832
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710 2 $a University of South Dakota. $b Chemistry. $3 1679392
773 0 $t Masters Abstracts International $g 49-02.
790 1 0 $a Koodali, Ranjit, $e advisor
790 1 0 $a Jiang, Chaoyang $e committee member
790 1 0 $a Mei, Dongming $e committee member
790 $a 0203
791 $a M.S.
792 $a 2010
856 4 0 $u http://pqdd.sinica.edu.tw/twdaoapp/servlet/advanced?query=1482791